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Liquid Chromatography-Mass Spectrometry Sample Preparation A 20 mg sample was weighed into a 1.5 mL EP tube, followed by the addition of two small steel beads and 400 L methanol-water (V:V = 4:1, containing L-2-chlorophenylalanine, 4 g/mL)

Rich oleocanthal and oleacein extra virgin olive oil and inflammatory and antioxidant status in people with obesity and prediabetes

PMID 16129424

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