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The organic content was analyzed using data-dependent auto LC-MS (maXis, Bruker Daltonics) coupled to an UHPLC ACQUITY (Waters) using reverse phase chromatography (CORTECS UPLC C18 column, 150 mm 2.1 mm ID 1.6 m, Waters Corporation) in both positive and negative electrospray modes

The EMA did not ban the peptide outright, but member states including Germany, France, and the Netherlands implemented customs seizures for personal imports exceeding research-plausible quantities

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doi:10.3233/JAD-2012-111728 166

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H.TononiG.et al (2017)